By Dehuai Zeng
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Additional resources for Materials, Mechatronics and Automation IV
Insets are the corresponding size distribution and HRTEM image. (b)Raman spectra of N, S:GQDs. X-ray photoelectron spectroscopy (XPS) was performed to determine the composition of the S, N:GQDs. As shown in Figure 2, the full scan XPS spectrum shows several peaks at 284, 533, 400, 227 and 164 eV, which corresponds to C1s, O1s, N1s, S2s and S2p, respectively. The other two peaks at 102 and 152 eV are cause by the silicon substrate. The results indicate that nitrogen and sulfer are doped into GQDs through the hydrothermal method.
Fig. 2-Cu after SO2 corrosion test for 24h based on JIS standard,(a)6hrs; (b)24hrs The chemical constitution of this corrosion product is listed in Table 1. At point 1, the concentration of Ni is higher than that of Au. At point 2, there is large quantity of O and S, and Au is not detected. Oxides of Ni and Cu are detected and sulfates of Ni and Cu are probably existed. It is indicated that element of Au is etched off and the corrosion degree is serious than point1. At point 3, the major component is element of Au and little S is detected.
A white porous solid polymer electrolyte was obtained after exposed to the ultraviolet light about 8 hours for volatile organic solvent and non-organic solvent at room temperature. Generally, 34 Materials, Mechatronics and Automation IV this solid polymer electrolyte was like a porous membrane and the thickness of the membrane is about 50 µm. The solid polymer electrolyte was then immersed in a lithium ion battery electrolyte solution under dry argon atmosphere in a glove box (MBRAUN, American).
Materials, Mechatronics and Automation IV by Dehuai Zeng