By Georgia S. Lemen, John P. Wolfe (auth.), Marc Taillefer, Dawei Ma (eds.)
Palladium-Catalyzed sp2C–N Bond Forming Reactions: contemporary advancements and purposes. Metal-catalyzed C(sp2)-N bond formation.- contemporary advancements in Recyclable Copper Catalyst structures for C−N Bond Forming Cross-Coupling Reactions utilizing Aryl Halides and Arylboronic Acids. meeting of N-containing heterocycles through Pd and Cu-catalyzed C-N bond formation reactions. Copper-Catalyzed C(aryl)-N Bond Formation.
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Extra resources for Amination and Formation of sp2 C-N Bonds
Aqueous KOH 3. Aqueous Acid 64% N Me O OH O O 75 N Me O F H N O N O N N N Me ZM549865 O Scheme 10 Large-Scale Synthesis of ZM549865 via Pd-Catalyzed N-Arylation 1. NaOH/ toluene 2. Pd(OAc)2, BINAP NaOtBu, toluene, 110 ºC 3. H2, Pd/C, H2O, AcOH 4. S. P. Wolfe Cl NH2 CN + CF3 1. 5 mol %) Cs2CO3, toluene, 80 ºC 2. H2SO4, H2O 75–79% O F3C NH2 N H Et O MeO CF3 N F3C N Et CF3 O Torcetrapib Scheme 13 Large-Scale Synthesis of Torcetrapib via Pd-Catalyzed N-Arylation 4-trifluoromethylaniline, which cannot be stored for long periods of time.
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Amination and Formation of sp2 C-N Bonds by Georgia S. Lemen, John P. Wolfe (auth.), Marc Taillefer, Dawei Ma (eds.)